TY - JOUR
T1 - Practical resolution of 3-phenyl-2H-azirine-2-methanol at very low temperature by using lipase immobilized on porous ceramic and optimized acylating agent
AU - Sakai, Takashi
AU - Matsuda, Akiko
AU - Korenaga, Toshinobu
AU - Ema, Tadashi
PY - 2003/9/1
Y1 - 2003/9/1
N2 - A synthetically useful primary alcohol, 3-phenyl-2H-azirine-2-methanol, was resolved efficiently by a reaction at -40 °C with a lipase immobilized on the porous ceramic (Toyonite) and vinyl butanoate in ether (E value of 130 and TTN/h value of 7800).
AB - A synthetically useful primary alcohol, 3-phenyl-2H-azirine-2-methanol, was resolved efficiently by a reaction at -40 °C with a lipase immobilized on the porous ceramic (Toyonite) and vinyl butanoate in ether (E value of 130 and TTN/h value of 7800).
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U2 - 10.1246/bcsj.76.1819
DO - 10.1246/bcsj.76.1819
M3 - Article
AN - SCOPUS:0141706533
SN - 0009-2673
VL - 76
SP - 1819
EP - 1821
JO - Bulletin of the Chemical Society of Japan
JF - Bulletin of the Chemical Society of Japan
IS - 9
ER -