Synthesis and structural determination of 1,1′-spirobi(3H-2,1-benzoxatellurole)-3-one ([10-Te-4(C2O2)]): Conversion of diacyloxyspirotellurane to alkoxyspirotellurane by reduction with lithium aluminium hydride

Yutaka Takaguchi, Naomichi Furukawa

Research output: Contribution to journalArticle

10 Citations (Scopus)

Abstract

Selective reduction of the diacyloxyspirotellurane 1 with lithium aluminium hydride gave the acyloxyalkoxyspirotellurane 2 and dialkoxyspirotellurane 3, respectively. The X-ray crystal structure analysis of 2 (R = 0.020) reveals distorted trigonal-bipyramidal geometry about tellurium, similar to structures previously determined for other spirotelluranes.

Original languageEnglish
Pages (from-to)365-366
Number of pages2
JournalChemistry Letters
Issue number5
DOIs
Publication statusPublished - 1996

ASJC Scopus subject areas

  • Chemistry(all)

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