Synthesis and characterization of gelatin-siloxane hybrids derived through sol-gel procedure

Lei Ren, Kanji Tsuru, Satoshi Hayakawa, Akiyoshi Osaka

Research output: Contribution to journalArticle

93 Citations (Scopus)

Abstract

A new type of inorganic-organic hybrid materials incorporating gelatin and 3-(glycidoxypropyl) trimethoxysilane (GPSM) was prepared through sol-gel processing. A solid-state 29Si NMR analysis indicated that all the methoxy silane groups of GPSM were polymerized to yield-Si-O-Si- bridging bonds. An amino acid analysis confirmed grafting reactions of GPSM against gelatin chains. The increasing GPSM/gelatin ratio stimulated gel formation, phase separation, and the density of GPSM-crosslinking of the gelatin chains as well as it changed the micro- and macro- structures and the viscoelastic properties of the final products.

Original languageEnglish
Article number333563
Pages (from-to)115-121
Number of pages7
JournalJournal of Sol-Gel Science and Technology
Volume21
Issue number1-2
DOIs
Publication statusPublished - Jan 1 2001

Keywords

  • Gelatin
  • Hybrid
  • Siloxane
  • Sol-gel method

ASJC Scopus subject areas

  • Electronic, Optical and Magnetic Materials
  • Ceramics and Composites
  • Chemistry(all)
  • Biomaterials
  • Condensed Matter Physics
  • Materials Chemistry

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