Preparation and characterization of β-Tricalcium phosphate powders with high solubility for chelate-setting calcium-phosphate cements

Kohei Nagata, Toshiisa Konishi, Michiyo Honda, Mamoru Aizawa

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Abstract

We have previously developed a novel chelate-setting β-Tricalcium phosphate (β-TCP) cement with non-fragmentation property in vivo. This novel cement has been set on the basis of chelate-setting mechanism of inositol phosphate (IP6). In this study, β-TCP powders were synthesized by mechanochemical method, and the as-prepared powders were heated at 600-1300°C for 1 h. Some properties of the resulting powders were examined. The crystalline phase of the resulting powders in the range of 600-1100°C was of β-TCP single phase. In the cases at 1200°C and 1300°C, the resulting powders were composed of β-TCP and α-TCP. Median particle sizes of the resulting powders increased with heating temperature from 5.35 μm up to 47.7 μm. Dissolution rate of Ca2+ ions from the β-TCP powders was measured by Japanese Industrial Standard T 0330-3. When the heating temperature was at 700°C, the Ca2+ ions solubility was the highest among examined samples. The β-TCP powder heated at 700°C for 1 h will be expected as the starting powder for paste-like artificial bone filler with excellent solubility.

Original languageEnglish
Title of host publicationBioceramics - 29th Symposium and Annual Meeting of the International Society for Ceramics in Medicine
PublisherTrans Tech Publications Ltd
Pages194-198
Number of pages5
Volume758 KEM
ISBN (Print)9783035712209
DOIs
Publication statusPublished - Jan 1 2017
Event29th Symposium and Annual Meeting of the International Society for Ceramics in Medicine, ISCM 2017 - Toulouse, France
Duration: Oct 25 2017Oct 27 2017

Publication series

NameKey Engineering Materials
Volume758 KEM
ISSN (Print)1013-9826

Other

Other29th Symposium and Annual Meeting of the International Society for Ceramics in Medicine, ISCM 2017
CountryFrance
CityToulouse
Period10/25/1710/27/17

Fingerprint

Calcium phosphate
Powders
Cements
Phosphates
Solubility
Ions
tricalcium phosphate
calcium phosphate
Heating
Inositol Phosphates
Ointments
Fillers
Bone
Dissolution
Particle size
Crystalline materials
Temperature

Keywords

  • Bone filler
  • Mechanochemical method
  • Solubility
  • β-Tricalcium phosphate

ASJC Scopus subject areas

  • Materials Science(all)
  • Mechanics of Materials
  • Mechanical Engineering

Cite this

Nagata, K., Konishi, T., Honda, M., & Aizawa, M. (2017). Preparation and characterization of β-Tricalcium phosphate powders with high solubility for chelate-setting calcium-phosphate cements. In Bioceramics - 29th Symposium and Annual Meeting of the International Society for Ceramics in Medicine (Vol. 758 KEM, pp. 194-198). (Key Engineering Materials; Vol. 758 KEM). Trans Tech Publications Ltd. https://doi.org/10.4028/www.scientific.net/KEM.758.194

Preparation and characterization of β-Tricalcium phosphate powders with high solubility for chelate-setting calcium-phosphate cements. / Nagata, Kohei; Konishi, Toshiisa; Honda, Michiyo; Aizawa, Mamoru.

Bioceramics - 29th Symposium and Annual Meeting of the International Society for Ceramics in Medicine. Vol. 758 KEM Trans Tech Publications Ltd, 2017. p. 194-198 (Key Engineering Materials; Vol. 758 KEM).

Research output: Chapter in Book/Report/Conference proceedingConference contribution

Nagata, K, Konishi, T, Honda, M & Aizawa, M 2017, Preparation and characterization of β-Tricalcium phosphate powders with high solubility for chelate-setting calcium-phosphate cements. in Bioceramics - 29th Symposium and Annual Meeting of the International Society for Ceramics in Medicine. vol. 758 KEM, Key Engineering Materials, vol. 758 KEM, Trans Tech Publications Ltd, pp. 194-198, 29th Symposium and Annual Meeting of the International Society for Ceramics in Medicine, ISCM 2017, Toulouse, France, 10/25/17. https://doi.org/10.4028/www.scientific.net/KEM.758.194
Nagata K, Konishi T, Honda M, Aizawa M. Preparation and characterization of β-Tricalcium phosphate powders with high solubility for chelate-setting calcium-phosphate cements. In Bioceramics - 29th Symposium and Annual Meeting of the International Society for Ceramics in Medicine. Vol. 758 KEM. Trans Tech Publications Ltd. 2017. p. 194-198. (Key Engineering Materials). https://doi.org/10.4028/www.scientific.net/KEM.758.194
Nagata, Kohei ; Konishi, Toshiisa ; Honda, Michiyo ; Aizawa, Mamoru. / Preparation and characterization of β-Tricalcium phosphate powders with high solubility for chelate-setting calcium-phosphate cements. Bioceramics - 29th Symposium and Annual Meeting of the International Society for Ceramics in Medicine. Vol. 758 KEM Trans Tech Publications Ltd, 2017. pp. 194-198 (Key Engineering Materials).
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