Potassium hydrogen trans-glutaconate monohydrate at 295, 245 and 40 K, and its rubidium analogue at 298 K

Setsou Kashino, Jun Ichiro Taka, Takeo Fukunaga, Hiroyuki Ishida

Research output: Contribution to journalArticle

4 Citations (Scopus)

Abstract

A centrosymmetric and short O-H···O hydrogen bond was found in isomorphic crystals of potassium hydrogen trans-glutaconate monohydrate (potassium hydrogen trans-pent-2-ene-1,5-dioate, K+·C5H5 O4-·H2O), (I), and rubidium hydrogen trans-glutaconate monohydrate (rubidium hydrogen trans-pent-2-ene-1,5-dioate, Rb+·C5H5 O4-·H2O), (II). The O···O distance at room temperature is 2.444 (3) Å in (I), and 2.417 (4) Å in (II). The O···O distance for (I) showed no significant decrease at low temperatures.

Original languageEnglish
Pages (from-to)549-552
Number of pages4
JournalActa Crystallographica Section C: Crystal Structure Communications
Volume57
Issue number5
DOIs
Publication statusPublished - May 2001

Fingerprint

Rubidium
rubidium
Hydrogen
potassium
Potassium
analogs
hydrogen
Temperature
Hydrogen bonds
hydrogen bonds
Crystals
glutaconic acid
room temperature
crystals

ASJC Scopus subject areas

  • Condensed Matter Physics
  • Structural Biology

Cite this

Potassium hydrogen trans-glutaconate monohydrate at 295, 245 and 40 K, and its rubidium analogue at 298 K. / Kashino, Setsou; Taka, Jun Ichiro; Fukunaga, Takeo; Ishida, Hiroyuki.

In: Acta Crystallographica Section C: Crystal Structure Communications, Vol. 57, No. 5, 05.2001, p. 549-552.

Research output: Contribution to journalArticle

@article{0d8520f7b3834086819b6a34c4b45f53,
title = "Potassium hydrogen trans-glutaconate monohydrate at 295, 245 and 40 K, and its rubidium analogue at 298 K",
abstract = "A centrosymmetric and short O-H···O hydrogen bond was found in isomorphic crystals of potassium hydrogen trans-glutaconate monohydrate (potassium hydrogen trans-pent-2-ene-1,5-dioate, K+·C5H5 O4-·H2O), (I), and rubidium hydrogen trans-glutaconate monohydrate (rubidium hydrogen trans-pent-2-ene-1,5-dioate, Rb+·C5H5 O4-·H2O), (II). The O···O distance at room temperature is 2.444 (3) {\AA} in (I), and 2.417 (4) {\AA} in (II). The O···O distance for (I) showed no significant decrease at low temperatures.",
author = "Setsou Kashino and Taka, {Jun Ichiro} and Takeo Fukunaga and Hiroyuki Ishida",
year = "2001",
month = "5",
doi = "10.1107/S0108270101003237",
language = "English",
volume = "57",
pages = "549--552",
journal = "Acta Crystallographica Section C: Crystal Structure Communications",
issn = "0108-2701",
publisher = "International Union of Crystallography",
number = "5",

}

TY - JOUR

T1 - Potassium hydrogen trans-glutaconate monohydrate at 295, 245 and 40 K, and its rubidium analogue at 298 K

AU - Kashino, Setsou

AU - Taka, Jun Ichiro

AU - Fukunaga, Takeo

AU - Ishida, Hiroyuki

PY - 2001/5

Y1 - 2001/5

N2 - A centrosymmetric and short O-H···O hydrogen bond was found in isomorphic crystals of potassium hydrogen trans-glutaconate monohydrate (potassium hydrogen trans-pent-2-ene-1,5-dioate, K+·C5H5 O4-·H2O), (I), and rubidium hydrogen trans-glutaconate monohydrate (rubidium hydrogen trans-pent-2-ene-1,5-dioate, Rb+·C5H5 O4-·H2O), (II). The O···O distance at room temperature is 2.444 (3) Å in (I), and 2.417 (4) Å in (II). The O···O distance for (I) showed no significant decrease at low temperatures.

AB - A centrosymmetric and short O-H···O hydrogen bond was found in isomorphic crystals of potassium hydrogen trans-glutaconate monohydrate (potassium hydrogen trans-pent-2-ene-1,5-dioate, K+·C5H5 O4-·H2O), (I), and rubidium hydrogen trans-glutaconate monohydrate (rubidium hydrogen trans-pent-2-ene-1,5-dioate, Rb+·C5H5 O4-·H2O), (II). The O···O distance at room temperature is 2.444 (3) Å in (I), and 2.417 (4) Å in (II). The O···O distance for (I) showed no significant decrease at low temperatures.

UR - http://www.scopus.com/inward/record.url?scp=0035338570&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=0035338570&partnerID=8YFLogxK

U2 - 10.1107/S0108270101003237

DO - 10.1107/S0108270101003237

M3 - Article

VL - 57

SP - 549

EP - 552

JO - Acta Crystallographica Section C: Crystal Structure Communications

JF - Acta Crystallographica Section C: Crystal Structure Communications

SN - 0108-2701

IS - 5

ER -