N,N'-Bis(3-nitrobenzylidene)-2,2'-[2-(3-nitrophenyl)imidazolidine-1, 3-di-yl]diethanamine

Mohammad Hossein Habibi, Narges Abarghooei-Shirazi, Yuki Yamane, Takayoshi Suzuki

Research output: Contribution to journalArticle

2 Citations (Scopus)

Abstract

The title compound, C27H27N7O6, a Schiff base, was synthesized by the reaction of triethyl-enetetra-mine with 3-nitro-benzealdehyde. There are two independent mol-ecules in the asymmetric unit. The central aromatic ring in one mol-ecule makes dihedral angles of 23.99 (7) and 20.06 (6)° with the two terminal rings; for the second mol-ecule, these angles are 26.14 (6) and 24.64 (6)°.

Original languageEnglish
JournalActa Crystallographica Section E: Structure Reports Online
Volume66
Issue number3
DOIs
Publication statusPublished - 2010

Fingerprint

Imidazolidines
Schiff Bases
Dihedral angle
rings
imines
dihedral angle

Keywords

  • Data-to-parameter ratio = 8.5
  • Mean σ(C-C) = 0.005 Å
  • R factor = 0.035
  • Single-crystal X-ray study
  • T = 193 K
  • WR factor = 0.100

ASJC Scopus subject areas

  • Condensed Matter Physics
  • Materials Science(all)
  • Chemistry(all)

Cite this

N,N'-Bis(3-nitrobenzylidene)-2,2'-[2-(3-nitrophenyl)imidazolidine-1, 3-di-yl]diethanamine. / Habibi, Mohammad Hossein; Abarghooei-Shirazi, Narges; Yamane, Yuki; Suzuki, Takayoshi.

In: Acta Crystallographica Section E: Structure Reports Online, Vol. 66, No. 3, 2010.

Research output: Contribution to journalArticle

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AU - Habibi, Mohammad Hossein

AU - Abarghooei-Shirazi, Narges

AU - Yamane, Yuki

AU - Suzuki, Takayoshi

PY - 2010

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N2 - The title compound, C27H27N7O6, a Schiff base, was synthesized by the reaction of triethyl-enetetra-mine with 3-nitro-benzealdehyde. There are two independent mol-ecules in the asymmetric unit. The central aromatic ring in one mol-ecule makes dihedral angles of 23.99 (7) and 20.06 (6)° with the two terminal rings; for the second mol-ecule, these angles are 26.14 (6) and 24.64 (6)°.

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KW - Data-to-parameter ratio = 8.5

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KW - R factor = 0.035

KW - Single-crystal X-ray study

KW - T = 193 K

KW - WR factor = 0.100

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