Monoprotonated [2.2.2]cryptand picrate monohydrate

Moamen S. Refat; Kazuma Gotoh; Hiroyuki Ishida

doi:10.1107/S1600536806036518

Monoprotonated [2.2.2]cryptand picrate monohydrate

Moamen S. Refat, Kazuma Gotoh, Hiroyuki Ishida

Research output: Contribution to journal › Article

1 Citation (Scopus)

Abstract

The title compound, 4,7,13,16,21,24-hexaoxa-1-azonia-10-azabicyclo[8.8.8] hexacosane picrate monohydrate, C₁₈H₃₇N₂O ₆⁺-C₆H₂N₃O ₇^-·H₂O, is a salt of [2.2.2]cryptand (4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]hexacosane) with picric acid (2,4,6-trinitrophenol). The monoprotonated cryptand cation encapsulates a water molecule through N-H⋯O and O-H⋯O hydrogen bonds.

Original language	English
Pages (from-to)	o4407-o4409
Journal	Acta Crystallographica Section E: Structure Reports Online
Volume	62
Issue number	10
DOIs	https://doi.org/10.1107/S1600536806036518
Publication status	Published - Oct 1 2006

ASJC Scopus subject areas

Chemistry(all)
Materials Science(all)
Condensed Matter Physics

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Refat, M. S., Gotoh, K., & Ishida, H. (2006). Monoprotonated [2.2.2]cryptand picrate monohydrate. Acta Crystallographica Section E: Structure Reports Online, 62(10), o4407-o4409. https://doi.org/10.1107/S1600536806036518

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abstract = "The title compound, 4,7,13,16,21,24-hexaoxa-1-azonia-10-azabicyclo[8.8.8] hexacosane picrate monohydrate, C18H37N2O 6+-C6H2N3O 7-·H2O, is a salt of [2.2.2]cryptand (4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]hexacosane) with picric acid (2,4,6-trinitrophenol). The monoprotonated cryptand cation encapsulates a water molecule through N-H⋯O and O-H⋯O hydrogen bonds.",

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AB - The title compound, 4,7,13,16,21,24-hexaoxa-1-azonia-10-azabicyclo[8.8.8] hexacosane picrate monohydrate, C18H37N2O 6+-C6H2N3O 7-·H2O, is a salt of [2.2.2]cryptand (4,7,13,16,21,24-hexaoxa-1,10-diazabicyclo[8.8.8]hexacosane) with picric acid (2,4,6-trinitrophenol). The monoprotonated cryptand cation encapsulates a water molecule through N-H⋯O and O-H⋯O hydrogen bonds.

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