High pressure generation in a kawai-type apparatus equipped with sintered diamond anvils

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Abstract

In this decade, attainable pressure range in a Kawai-type high-pressure apparatus equipped with sintered diamond as second stage anvil is significantly increased and we generated pressure to 97.2 GPa measured by in situ X-ray observation at SPring-8. By using this technique, we measured compressibility of (Fe0.08Mg0.92)SiO3 perovskite up to more than 90 GPa. The bulk modulus and its pressure derivative are determined to be 268 GPa and 3.8, respectively. These values are slightly different from previous results. However, we obtained consistent results with previous study of bulk modulus of 257 GPa and pressure derivative of 4.3 when we fitted the data in the pressure range less than 70 GPa. The change of compressibility may indicate the spin transition in Fe-bearing perovskite around 70 GPa as suggested by previous study, for example, electrical conductivity measurement, X-ray emission method and so on.

Original languageEnglish
Pages (from-to)272-277
Number of pages6
JournalReview of High Pressure Science and Technology/Koatsuryoku No Kagaku To Gijutsu
Volume21
Issue number4
DOIs
Publication statusPublished - 2011

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Diamond
anvils
Diamonds
diamonds
bulk modulus
compressibility
Compressibility
Perovskite
Bearings (structural)
Elastic moduli
Derivatives
X rays
x rays
electrical resistivity

Keywords

  • Compressibility
  • Kawai-type multianvil apparatus
  • Perovskite
  • Pressure generation
  • Sintered diamond anvil

ASJC Scopus subject areas

  • Condensed Matter Physics
  • Materials Science(all)
  • Chemistry(all)

Cite this

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title = "High pressure generation in a kawai-type apparatus equipped with sintered diamond anvils",
abstract = "In this decade, attainable pressure range in a Kawai-type high-pressure apparatus equipped with sintered diamond as second stage anvil is significantly increased and we generated pressure to 97.2 GPa measured by in situ X-ray observation at SPring-8. By using this technique, we measured compressibility of (Fe0.08Mg0.92)SiO3 perovskite up to more than 90 GPa. The bulk modulus and its pressure derivative are determined to be 268 GPa and 3.8, respectively. These values are slightly different from previous results. However, we obtained consistent results with previous study of bulk modulus of 257 GPa and pressure derivative of 4.3 when we fitted the data in the pressure range less than 70 GPa. The change of compressibility may indicate the spin transition in Fe-bearing perovskite around 70 GPa as suggested by previous study, for example, electrical conductivity measurement, X-ray emission method and so on.",
keywords = "Compressibility, Kawai-type multianvil apparatus, Perovskite, Pressure generation, Sintered diamond anvil",
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AU - Yamazaki, Daisuke

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AB - In this decade, attainable pressure range in a Kawai-type high-pressure apparatus equipped with sintered diamond as second stage anvil is significantly increased and we generated pressure to 97.2 GPa measured by in situ X-ray observation at SPring-8. By using this technique, we measured compressibility of (Fe0.08Mg0.92)SiO3 perovskite up to more than 90 GPa. The bulk modulus and its pressure derivative are determined to be 268 GPa and 3.8, respectively. These values are slightly different from previous results. However, we obtained consistent results with previous study of bulk modulus of 257 GPa and pressure derivative of 4.3 when we fitted the data in the pressure range less than 70 GPa. The change of compressibility may indicate the spin transition in Fe-bearing perovskite around 70 GPa as suggested by previous study, for example, electrical conductivity measurement, X-ray emission method and so on.

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