Diffractometer for synchrotron radiation structural studies of high temperature melts

F. Marumo, H. Morikawa, Y. Shimizugawa, M. Tokonami, M. Miyake, K. Ohsumi, S. Sasaki

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A diffractometer has been constructed for structural studies of high-temperature melt with synchrotron radiation. It was designed to measure diffracted intensities from the free surface of a molten sample by scanning a scintillation counter with a fixed glancing angle of the incident beam. In order to heat samples up to 1500 °C, a small electric furnace is attached to the diffractometer. It carries a hemicircular (100 mm in diameter) cover, which has a window for the passage of x rays. The window is covered with a Kapton film. The sample container made of 30 Rh-Pt is mounted at the center of the furnace. A test measurement was performed on GeO2. Monochromatic beams with λ = 1.32 A and its second harmonics were taken out of synchrotron radiation by a β-alumina crystal (d002 = 11.3 A) and used as incident beams. To partial scattering curves obtained with λ and λ/2 were combined to a single curve after correction for absorption. The radial distribution function obtained from these data is in good agreement with that previously reported which was derived from diffraction data collected on a conventional diffractometer.

Original languageEnglish
Pages (from-to)2421-2424
Number of pages4
JournalReview of Scientific Instruments
Issue number7
Publication statusPublished - Dec 1 1989

ASJC Scopus subject areas

  • Instrumentation

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    Marumo, F., Morikawa, H., Shimizugawa, Y., Tokonami, M., Miyake, M., Ohsumi, K., & Sasaki, S. (1989). Diffractometer for synchrotron radiation structural studies of high temperature melts. Review of Scientific Instruments, 60(7), 2421-2424. https://doi.org/10.1063/1.1140735