A Facile Synthesis of α,α-Difluoroalkyl Ethers and Carbonyl Fluoride Acetals by Oxidative Desulfurization-Fluorination

Manabu Kuroboshi, T. Hiyama

Research output: Contribution to journalArticlepeer-review

32 Citations (Scopus)

Abstract

α,α-Difluoro ethers and carbonyl fluoride acetals were readily prepared from thiocarboxylic O-acid esters and O, O′-disubstituted thiocarbonate, respectively, in moderate to good yields by the action of tetrabutylammonium dihydrogentrifluoride and N-bromosuccinimide or N-iodosuccinimide.

Original languageEnglish
Pages (from-to)251-252
Number of pages2
JournalSynlett
Volume1994
Issue number4
DOIs
Publication statusPublished - Apr 1 1994
Externally publishedYes

ASJC Scopus subject areas

  • Organic Chemistry

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